1,10-Phenanthroline is a heterocyclic organic compound. It is a white solid that is soluble in organic solvents. The 1,10 refers to the location of the nitrogen atoms that replace CH's in the hydrocar
Grignard reagents or Grignard compounds are chemical compounds with the general formula RMgXn, where X is a halide, R is an organic group, S is an ether, and n is usually 2. Usually, the ether groups
1,10-Phenanthroline
…determined by treatment of such reagents with small amounts of phenanthroline (ca. 1 mg) followed by titration with alcohols to a colourless endpoint. Grignard reagents may be similarly titrated. Phenanthroline is used in biochemical and pharmacological research as an inhibitor of the deubiquitination enzyme Rpn11…
Magnesium turnings are placed in a flask.
Tetrahydrofuran and a small piece of iodine are added.
A solution of alkyl bromide is added while heating.
After completion of the addition, the mixture is heated for a while.